Spectroscopy Problem Sets
 
These problems in structure elucidation are designed to help you during the Chemistry 719-721 sequence (second year organic chemistry for chemistry, biology, pre-med, pre-pharmacy, etc.).  You will need the free Adobe Acrobat Reader to view spectra.
 
 
Unknown #1 - C2H3Cl3  Unknown #8 - C4H10O  Unknown #15 - C5H10O
Unknown #2 - C2H4Cl2  Unknown #9 - C4H11N  Unknown #16 - C14H10O2
Unknown #3 - C4H10O  Unknown #10 - C7H6O  Unknown #17 - C13H12O
Unknown #4 - C3H8O  Unknown #11 - C15H14O  Unknown #18 - C6H10O
Unknown #5 - C8H8O  Unknown #12 - C13H10O  Unknown #19 - C5H8O2
Unknown #6 - C5H10O  Unknown #13 - C8H8O  Unknown #20 - C14H28O2
Unknown #7 - C3H9N  Unknown #14 - C7H5ClO  Unknown #21 - C8H8O2
     
 
 
Completed as part of Honors 719-721 Organic Chemistry by Chris Gabriel, Adam Freeman, and Alok Makam.

Thanks to the NMR archive at Pacific Lutheran University for some of the 1H and 13C NMR data and the NIST Webbook for some of the IR and Mass spectral data ("IR and Mass Spectra" by NIST Mass Spec Data Center, S.E. Stein, director, NIST Standard Reference Database Number 69, Eds. W.G. Mallard and P.J. Linstrom, August 1997, National Institute of Standards and Technology, Gaithersburg MD, 20899 (http://webbook.nist.gov).